The application of polymer matrix composites has found valuable in many engineering fields like electrical, marine, aerospace, electronics and microelectronics. Thus, a new technique like microwave through electromagnetic energy was explored for processing of polymer matrix composite. The roles of microwave in the post curing of polymer matrix composites cannot be underestimated, as it has the capacity to improve the mechanical and micro-structural properties of the composite produced. The aim of the study is to investigate the effect of microwave post curing on the mechanical and micro-structural properties of particulate reinforced polymer matrix composites. These effects were compared with composites post cured using conventional autoclave oven with the objective of investigating the significance of microwave curing on the tensile strength and structural qualities in terms of defects of the produced composites. A specific study comprising of aluminum filled polyester based composite and carbon black filled polyester based composite were investigated using two different composite curing methods (microwave oven and conventional autoclave oven). The investigation, through experimentation was based on mechanical property (tensile strength) and micro-structural quality (defects) of the produced composites. Comparing the results of the post-curing of the composites using microwave and conventional methods, there is direct relationship between the tensile strength and the percentage weight fraction of the fillers with respect to the post curing methods. 30% aluminium filled, post cured in microwave has 0.01 MPa tensile strength, 20% aluminium filled (microwave) has 0.0076MPa while 30% aluminium filled (conventional oven curing) has 0.0092MPa and 20% aluminium filled (conventional oven curing) has 0.0068MPa. Also, composites post-cured with microwave show less voids defect compared to that post-cured by conventional autoclave oven. It was shown in this paper that post-curing of the particulate composites through microwave was able to improve the tensile strength and minimize defects better as compared to conventional autoclave method.
Published in | Advances in Materials (Volume 4, Issue 5) |
DOI | 10.11648/j.am.20150405.11 |
Page(s) | 85-94 |
Creative Commons |
This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited. |
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Copyright © The Author(s), 2015. Published by Science Publishing Group |
Autoclave, Curing, Micro-Structure, Microwave, Polymer Matrix Composites, Tensile Strength
[1] | Kwack M., Robinson P., Bismarck A., Wise R., (2011). Curing of composite materials using the recently developed Haphaistos microwave. 18th International Conference on composites materials, Korea, Aug. 21-26 |
[2] | Hussein Mohammed (2012). The effect of curing time on the mechanical properties of polyester reinforced aluminum particulate composite. Nahrain University college of Engineering Journal. Vol. 15, No 2, pp 197-225 |
[3] | Hertzberg R.W., (1989). Deformation and fracture mechanics of engineering materials”, 3rd ed., John Wiley & Sons |
[4] | Sunain Katoch, Vinay Sharma, P. P. Kundu, (2010). Swelling Kinetics of unsaturated polyester layered silicate nanocomposite depending on the fabrication Mmethod”, The Open-Access Journal for the Basic Principles of Diffusion Theory, Experiment and Application, 13(1), pp 1-31 |
[5] | Grayson M and Eckroth, D Ed., (1982). Encyclopedia of chemical technology”, 3rd ed., Vol 18, John Wiley & Sons, p 575 |
[6] | Philip C. Sturman and Rexford N. Y. (1999). Induction Heating of Polymer Matrix Composite Fibre Strands. SAMPE Journal, Vol. 26, No 4 |
[7] | Das S, Mukhopadhyay A K, Datta S and Basu D (2009) Bull. Mater. Sci., Vol. 32, No. 1 |
[8] | Daniel B. Miracle and Steven L. Donaldson were the Volume Chairs, (2001). Asm Hand Book, Volume 21, Composite, ASM International Handbook Committee, |
[9] | Dominick V Rsato and Donal V Rosat, (2003). Plastics Engineering Products Design”, Elsevier Ltd, The Boulevard, Langford Lane, Kidlington, Oxford OX5 lGB, UK, p 5 |
[10] | Sutton, W.H. (1989). Microwave Processing of Ceramics, Ceramic Bulletin, 68(2), 376-86 |
[11] | Das S, Mukhopadhyay A K, Datta S and Basu D (2008b) (communicated) |
[12] | Nightingale, C (2000). Microwave assisted curing of epoxy resins and composites”, PhD Thesis. University of Manchester, UK |
[13] | Lee, W and Springer, G (1984). Microwave curing of composite. Journal of Composite Materials, Vol.18, No.4, pp 387-409 |
[14] | Wei, J., Chang, Y., Thomas, B and Hawley, M (1991). Microwave Heating of Thick-Section Graphite Fiber/Epoxy Composite. Proceedings of ICCM-8, Vol.1, pp10-L-1 to 10-L-10 |
[15] | Boey, F and Lee, T (1991). Electromagnetic Radiation Curing of an Epoxy/Fibre Glass Reinforced Composit, Radiation Physics and Chemistry, Vol.38, No.4, pp 419-42 |
[16] | Yue, C and Boey, F (1993). The Effect of Microwave and Thermal Curing on the Interfacial Properties of an Epoxy/Glass Composite. 2nd International Conference on the Deformation and Fracture of Composites, pp. 121-128 |
[17] | Akay, M and Kong Ah Mun, (1995). Bearing strength of autoclave and oven cured Kevlar/epoxy laminates under static and dynamic loading, Composites, 26, pp.451-456, (Receive August 1994; revised 7 October 1994) |
[18] | Jian Zhou, Chun Shi, Bingchu Mei, Runzhang Yuan, Zhengyi Fu, (2003). Research on the technology and the mechanical properties of the microwave processing of polymer, Journal of Materials Processing Technology, 137, pp 156-158 |
[19] | Bambang Soesatyo, Aaron Blicblau, Elias Siores, (1999). Effect of rapid curing doped epoxy adhesive between two polycarbonate substrates on the bond tensile strength”, Journal of Materials Processing Technology, 89(90), pp.451-456 |
[20] | Bai, S. L., Djafari, V., Andreani, M and Francois, D (1995). A comparative study of the mechanical behaviour of an epoxy resin cured by Microwaves with one cured thermally”, European. Polymer Journal, 31, (9), pp.875-884. (Received 17 January 1994; accepted in final form 27 June 1994) |
[21] | Chaowasakoo, T., Sombatsompop, S., (2007). Mechanical and morphological properties of fly ash/epoxy composites using conventional thermal and microwave curing method. Composites Science and Technology, 67, pp.2282-2291 |
[22] | Islam R. A and Chan Y. C. (2003). Effect of Microwave Preheating on the Bonding Performance of Flip chip on Flex Joint. Micro electronics Reliability. Vol. 44, pp 815-821 |
[23] | Bai, S. L., and Djafari, V (1995). Interfacial properties of microwave cured Composites, Composites, 26, pp.645-651 |
[24] | Adefemi O. Adeodu, Christopher O. Anyaeche, Oluleke O. Oluwole, Charles U. Omohimoria (2015). Effect of Microwave and Conventional Heating on the Cure Cycles of Particulate Reinforced Polymer Matrix Composites. International Journal of Materials Science and Applications. Vol. 4, No. 4, pp. 229-240 |
[25] | Hossain M. R., Hossain M. F., Islam M. A., (2014). Effect of wood properties on the behaviors of wood particle reinforced polymer matrix composites. J. Sci. Res 6(3) Page 431-443 |
[26] | Azuke F., Aigbodion V. S., Abdulwahab M., Fayomi O. S.I., Popoola A. P.I., Nwoyi C. I., Garba B, (2012). Effect of bone particle on the properties and microstructure of polypropylene-bone ash particulate composites. Results in Physics 2 Page 135-141 |
[27] | Chawla Nikhilesh and Yu Linshen (2001). Mechanical behavior of particle reinforced metal matrix composites. Advanced Engineering Material Vol. 6, page 1438-1656 |
[28] | Shao-Yunfu, Xi-Qiao Feng, Bernd Lauke, Yiu-wing Mail (2008). Effect of particle size particle-matrix interface adhesion and particle loading on mechanical properties of particulate-polymer composites. Science Direct. Composites: part B, 39 Page 933-961 |
[29] | Hassan S. B., Oghenevweta E. J., Aigbodion V. S (2012). Potential of maize stalk ash as reinforcement in polyester composites. Journal of Minerals Materials Characterization and Engineering. Vol. 11, No 4, Page 445-459 |
[30] | Upadhyaya D D, Ghosh A, Gurumurthy K R and Prasad R (2001) Ceram. Int. 27 415 |
[31] | Nikki Sgriccia and Hawley M. C. (2007). Thermal Morphological and Electrical Characterization of Microwave Processed Natural Fibre Composites. Composites Science and Technology. Vol. 67, pp 1986-1991 |
[32] | Yizhuo Gu, Min Li, Zuoguang Zhang and Zhijie Sun, (2012). Measuring Methods and Process Analysis of Void Formation Conditions for Resin Matrix Composites. Laboratory of Aerospace Materials and Performance. Beijing 100191, China |
[33] | Das S, Mukhopadhyay A K, Datta S and Basu D (2005) Trans. Ind. Ceram. Soc. 64 143 |
APA Style
Adeodu Adefemi, Anyaeche Christopher, Oluwole Oluleke, Alo Oluwaseun. (2015). Effect of Microwave and Conventional Autoclave Post-Curing on the Mechanical and Micro-structural Properties of Particulate Reinforced Polymer Matrix Composites. Advances in Materials, 4(5), 85-94. https://doi.org/10.11648/j.am.20150405.11
ACS Style
Adeodu Adefemi; Anyaeche Christopher; Oluwole Oluleke; Alo Oluwaseun. Effect of Microwave and Conventional Autoclave Post-Curing on the Mechanical and Micro-structural Properties of Particulate Reinforced Polymer Matrix Composites. Adv. Mater. 2015, 4(5), 85-94. doi: 10.11648/j.am.20150405.11
AMA Style
Adeodu Adefemi, Anyaeche Christopher, Oluwole Oluleke, Alo Oluwaseun. Effect of Microwave and Conventional Autoclave Post-Curing on the Mechanical and Micro-structural Properties of Particulate Reinforced Polymer Matrix Composites. Adv Mater. 2015;4(5):85-94. doi: 10.11648/j.am.20150405.11
@article{10.11648/j.am.20150405.11, author = {Adeodu Adefemi and Anyaeche Christopher and Oluwole Oluleke and Alo Oluwaseun}, title = {Effect of Microwave and Conventional Autoclave Post-Curing on the Mechanical and Micro-structural Properties of Particulate Reinforced Polymer Matrix Composites}, journal = {Advances in Materials}, volume = {4}, number = {5}, pages = {85-94}, doi = {10.11648/j.am.20150405.11}, url = {https://doi.org/10.11648/j.am.20150405.11}, eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.am.20150405.11}, abstract = {The application of polymer matrix composites has found valuable in many engineering fields like electrical, marine, aerospace, electronics and microelectronics. Thus, a new technique like microwave through electromagnetic energy was explored for processing of polymer matrix composite. The roles of microwave in the post curing of polymer matrix composites cannot be underestimated, as it has the capacity to improve the mechanical and micro-structural properties of the composite produced. The aim of the study is to investigate the effect of microwave post curing on the mechanical and micro-structural properties of particulate reinforced polymer matrix composites. These effects were compared with composites post cured using conventional autoclave oven with the objective of investigating the significance of microwave curing on the tensile strength and structural qualities in terms of defects of the produced composites. A specific study comprising of aluminum filled polyester based composite and carbon black filled polyester based composite were investigated using two different composite curing methods (microwave oven and conventional autoclave oven). The investigation, through experimentation was based on mechanical property (tensile strength) and micro-structural quality (defects) of the produced composites. Comparing the results of the post-curing of the composites using microwave and conventional methods, there is direct relationship between the tensile strength and the percentage weight fraction of the fillers with respect to the post curing methods. 30% aluminium filled, post cured in microwave has 0.01 MPa tensile strength, 20% aluminium filled (microwave) has 0.0076MPa while 30% aluminium filled (conventional oven curing) has 0.0092MPa and 20% aluminium filled (conventional oven curing) has 0.0068MPa. Also, composites post-cured with microwave show less voids defect compared to that post-cured by conventional autoclave oven. It was shown in this paper that post-curing of the particulate composites through microwave was able to improve the tensile strength and minimize defects better as compared to conventional autoclave method.}, year = {2015} }
TY - JOUR T1 - Effect of Microwave and Conventional Autoclave Post-Curing on the Mechanical and Micro-structural Properties of Particulate Reinforced Polymer Matrix Composites AU - Adeodu Adefemi AU - Anyaeche Christopher AU - Oluwole Oluleke AU - Alo Oluwaseun Y1 - 2015/10/10 PY - 2015 N1 - https://doi.org/10.11648/j.am.20150405.11 DO - 10.11648/j.am.20150405.11 T2 - Advances in Materials JF - Advances in Materials JO - Advances in Materials SP - 85 EP - 94 PB - Science Publishing Group SN - 2327-252X UR - https://doi.org/10.11648/j.am.20150405.11 AB - The application of polymer matrix composites has found valuable in many engineering fields like electrical, marine, aerospace, electronics and microelectronics. Thus, a new technique like microwave through electromagnetic energy was explored for processing of polymer matrix composite. The roles of microwave in the post curing of polymer matrix composites cannot be underestimated, as it has the capacity to improve the mechanical and micro-structural properties of the composite produced. The aim of the study is to investigate the effect of microwave post curing on the mechanical and micro-structural properties of particulate reinforced polymer matrix composites. These effects were compared with composites post cured using conventional autoclave oven with the objective of investigating the significance of microwave curing on the tensile strength and structural qualities in terms of defects of the produced composites. A specific study comprising of aluminum filled polyester based composite and carbon black filled polyester based composite were investigated using two different composite curing methods (microwave oven and conventional autoclave oven). The investigation, through experimentation was based on mechanical property (tensile strength) and micro-structural quality (defects) of the produced composites. Comparing the results of the post-curing of the composites using microwave and conventional methods, there is direct relationship between the tensile strength and the percentage weight fraction of the fillers with respect to the post curing methods. 30% aluminium filled, post cured in microwave has 0.01 MPa tensile strength, 20% aluminium filled (microwave) has 0.0076MPa while 30% aluminium filled (conventional oven curing) has 0.0092MPa and 20% aluminium filled (conventional oven curing) has 0.0068MPa. Also, composites post-cured with microwave show less voids defect compared to that post-cured by conventional autoclave oven. It was shown in this paper that post-curing of the particulate composites through microwave was able to improve the tensile strength and minimize defects better as compared to conventional autoclave method. VL - 4 IS - 5 ER -